Quantitative Microscopy: (ii) manually estimate the grain size and grain boundary surface area per unit volume of a single-phase polycrystal

Note: This is a VR experiment, so idea is to play with the variables. Suggested steps, to utilize the simulation and learn from the changes, are:

  1. Select a microstructure and from its scale bar, try to get a rough estimate on the grain size of the sample. This will allow you to get a feel of how close the grain size analysis method provide the result.

  2. Measure the grain size using ASTM method. Herein, get the microstructure, and then obtain the number of grains at 100ร— magnification in 1 in2 area. First, obtain the ASTM grain size (n) using the equation:
    N=2n-1 ,
    where N is the number of grains at 100x in 1 in2 area.

Then, change the magnification (to start with, say 50ร—, or 200ร—). Accordingly, at 200ร—, one will obtain one-fourth (1/4th) number of the grains as the magnification has increased (both in x and y direction). Then check how the values change.

  1. For Jeffries method, utilize a circle with an area of 5000 mm2 and count the number of grains. Now, obtain the number of grains per mm2 (NA) as per the following equation:

N๐ด=๐‘€2/5000 x (๐‘›1+๐‘›2/2)
where n1 is the number of full grains, n2 is the number of grains intersected at circumference, and M is the magnification. The value of 5000 in the denominator corresponds to area of 5000 mm2 (of circle) where the grains are captured.

Now average grain area (ฤ€), with units of mm2, is obtained as 1/NA, and an average grain area in ยตm2 is given as :

ฤ€ (ยตm2) = 106/NA

Correspondingly, the mean diameter (d) can be given as:
dฬ„(๐œ‡๐‘š)= (๐ดฬ…)1/2 = 103/NA1/2

  1. In the grain boundary triple points (P) method, the triple points in an area are counted with quadruple points (where four grains meet) are accounted a weight of โ€˜twoโ€™. Accordingly, the number of grains per unit area (NA) is calculated using the equation:

NA = (๐‘ƒ/2 + 1) / AT

where AT is the area at 1ร— magnification, and the corresponding ASTM grain size, (n) is obtained as:
n = 3.322log ((๐‘ƒ/2 + 1) / AT) - 2.95

  1. Compare the grain size values obtained from various methods.