Estimation of precipitate size in age hardenable aluminium alloys
- Take TEM images
- Using ImageJ first set the scale bar
- Measure the length of precipitates using line measurement in ImageJ
- Assume sample thickness is of the order of 70 nm
- Correct the measured precipitate size using equation (1)
Example: Plate-like T1 (Al2CuLi) precipitate in Al-Cu-Li alloys as shown in figure 1.
Figure 1: (a) Plate-like T1 precipitate in Al-Cu-Li alloy. (b) Precipitates which were used to calculate the diameter of plate-like precipitates .
Table 1: Measured diameter of the marked red colour precipitates.
S. No. | Measured diameter (nm) | Corrected diameter (nm) |
---|---|---|
1 | 98.68 | 113.84 |
2 | 102.65 | 118.703 |
3 | 85.58 | 97.846 |
4 | 86.19 | 98.594 |
5 | 65.89 | 74.089 |
6 | 76.91 | 87.34 |
7 | 82.96 | 94.66 |
8 | 57.56 | 64.15 |
9 | 84.57 | 96.63 |
10 | 54.87 | 60.98 |
11 | 54.60 | 60.73 |
12 | 42.666 | 46.68 |