Determination of Particle Size and Particle Size Distribution Using Sieving Method
Materials Required
- Set of standard sieves (e.g., 10 to 325 mesh)
- Granular sample (e.g., sand, starch, or pharmaceutical powder)
- Weighing balance (accuracy ±0.01 g)
- Mechanical sieve shaker / manual setup
- Brush (for cleaning sieves)
- Collection pan
- Stopwatch or timer
- Calculator / spreadsheet for analysis
Procedure
- Arrange the sieves in descending order (coarsest on top, finest at bottom).
- Weigh approximately 100 g of the dry sample.
- Place a collection pan under the bottom sieve.
- Transfer the sample to the top sieve and secure the lid.
- Shake manually or mechanically for 10–15 minutes.
- Carefully remove and weigh the material retained on each sieve.
- Record the weights and calculate:
- Percentage retained = (Weight retained / Total weight) × 100
- Cumulative % passing = 100 – Cumulative % retained
- Plot a graph of log particle size (X-axis) vs. % finer (Y-axis).
- Determine D₁₀, D₅₀, and D₉₀ from the curve.
Observation and data
| Sieve No. | Aperture Size (µm) | Weight Retained (g) | % Retained | Cumulative % Retained | % Finer |
|---|---|---|---|---|---|
| 10 | 1700 | ||||
| 16 | 1000 | ||||
| 22 | 710 | ||||
| 25 | 600 | ||||
| 30 | 500 | ||||
| 36 | 425 | ||||
| 60 | 250 | ||||
| 85 | 180 | ||||
| 100 | 150 | ||||
| Pan | <150 |
Calculations
- Percentage Retained = (Weight Retained / Total Weight) × 100
- Cumulative % Passing = 100 – Cumulative % Retained
- Graphically determine D₁₀, D₅₀, and D₉₀ from the plotted curve.
Result
The particle size distribution was successfully determined, and the D₁₀, D₅₀, and D₉₀ values were obtained from the graph, reflecting the range and uniformity of the sample’s particle sizes.
Precautions
- Ensure sieves are clean and dry before use.
- Avoid overloading sieves.
- Maintain consistent shaking duration and motion.
- Handle sieves gently to prevent mesh damage.