Electrogravimetric Estimation of Metals
Materials Required:
- Magnetic stirrer
- Stopwatch
- Ammeter
- Voltmeter
- Rheostat
- Switch
- Alkaline Battery
- Beaker
- Pt gauze cathode
- Pt spiral anode
- Electrolytes Used: CuSO4, PbSO4, MnSO4, NiSO4, CdSO4
Procedure:
- Select the solution.
- Choose the cathode.
- Choose the anode.
- Select the voltage.
- Select the resistance.
- Select the time.
- Click on the start button.
- Note the total weight of cathode.
- Determine the mass of metal deposited.
Observations and Calculations:
Initial weight of the cathode = 10 g
Final weight of the cathode = ............... g
Amount of metal deposited (m) = ............... g
Voltage used = ............... V
Resistance used = ............... Ω
Current (I = V / R) = ............... A
Time taken for complete deposition (t) = ............... sec
Result:
The amount of metal deposited on the electrode = ............... g
Points to Remember while Performing the Experiment:
- Wear lab coat and gloves in the lab.
- Switch on the exhaust fan when entering the lab.
- Check if chemicals and reagents are available; prepare if not.
- Clean all apparatus with chromic acid and distilled water.
- Ensure apparatus are dry before use.
- Calibrate the weighing balance before measurements.
- Ensure voltmeter, ammeter, and rheostat work properly.
- Clean glassware with soap and distilled water.
- Recap reagent bottles after use.
- Switch off light, exhaust fan, and gas cylinder before leaving.
- Dispose of used gloves in a waste bin.