Instructions :-
lets start the experiment
![](images/durgesh lab edits.png)
![](images/heater.png)
![](images/heater-done.png)
stopwatch 4x >>
00
:
00
![](images/rotary.png)
![](images/empty-pippete.png)
![](images/pippete.png)
![](images/drop.png)
![](images/empty-flask.png)
![](images/oil sample.png)
![](images/hcl-half.png)
![](images/hcl-neck.png)
![](images/hcl.png)
![](images/koh 100ml.png)
![](images/koh 100ml-half.png)
![](images/koh 100ml-neck.png)
![](images/funnel.png)
![](images/empty-Burette-50ml.png)
![](images/Burette-20ml.png)
![](images/Burette-27ml.png)
![](images/Burette-50ml.png)
![](images/phenolphthelein-cap.png)
![](images/normal koh 15ml.png)
![](images/koh 15ml -phenolphthelien.png)
![](images/koh 15ml oil added.png)
![](images/koh 15ml oil added-phenolphthelien.png)
![](images/phenolphthelein-bottle.png)
Heat the oil mixture for 30 minutes at 700C to make oil proper soluble in KOH
S. No. | Weight of the oil taken (in g) |
Volume of 0.5 N HCL required to titrate (Vo) (in mL) |
Volume of 0.5 N HCL required to titrate the control (i.e. without oil) (Vc) (in mL) |
Weight of KOH required to complete the saponification (in mg)$ |
Saponification value (mg of KOH/g of oil) |
---|---|---|---|---|---|
1 | 1.51 | 7.3 | 20.1 | 359.04 | 237.77 |
2 | 1.50 | 7.5 | 20.0 | 350.62 | 233.75 |
3 | 1.53 | 7.0 | 20.2 | 370.26 | 242.00 |
Average | NA | NA | NA | NA | 237.84 |