Next click on "Dock the SPR sensor chip" button to enable "Open sensor chip door" button. Click on "Open sensor chip door"
button.
Now click on the Sensor chip image. After sensor chip is placed in the machine, click on
the "Close"
button.
Check all the composition required for preparing buffer. Click on "Primer with buffer"
button.
Part 2: Ligand Immobilization
Click on "EDC" and "NHS" checkboxes in step 4 and on button "Reagents" for sample
preparation.
Click on "Ligand" and "Sodium acetate buffer pH>3.5" checkboxes in step 4 and on button
"Sample preparation" for sample preparation.
Click on the "Ethanolamine" checkbox in step 4.
Now click on the "Open sample tray door" button in step 4.
Next click on "Eject tray plate" button. Once the plate comes out
from the SPR machine, click on the sample tray image.
Click on the
"Inject tray plate" button.
Click on the "Close sample tray door" button in step 4.
Click on "Start ligand immobilization" button to see the Ligand Immobilization.
Part 3: Interaction Analysis
Now click on the "Open sample tray door" button in step 5.
Next click on "Eject tray plate" button. Once the plate comes out form
from the SPR machine, click on the "Remove EDC, NHS and
ethanolmine sample tubes" button.
Click on both the checkboxes in step 5 and on button "Sample preparation".
Click on the
"Inject tray plate" button.
Click on the "Close sample tray door" button in step 5.
Click on "Inject analyte" button to see the Interation analysis.
Click on "Inject buffer" button.
Part 4: Regeneration Phase
Click on "Glycine pH 1-3" checkbox to remove remaining bound analyte.
Part 5: Test run and Concentration- dependent analysis
Click on "Test run" and "Concentration- dependent analysis" button.
Note: To repeat the experiment, click on the "Re-Do the Experiment" button.
Input Panels
Step 1
Step 2
Dock the SPR sensor
chip
Step 3
Step 4
Step 5
Step 6
Step 7
Covalent immobilization using amine coupling method
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